UPSC MainsANI-HUSB-VETER-SCIENCE-PAPER-II202510 Marks150 Words
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Q19.

Discuss the following in about 150 words each: 5.(b) Neutralization of cream.

How to Approach

The answer should begin by defining cream neutralization and its primary objectives in dairy processing, especially for butter making. The body will delve into the types of neutralizers used, the methods of their application, and the specific chemical reactions involved. It's crucial to mention the importance of calculating the correct amount of neutralizer and maintaining desired pH levels for product quality and shelf life. Conclude with the overall impact on dairy product quality.

Model Answer

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Introduction

Neutralization of cream is a crucial step in dairy processing, particularly in butter manufacturing, where raw cream often develops acidity due to the conversion of lactose into lactic acid by bacterial action. This acidity, if not controlled, can negatively impact the flavor, texture, and shelf-life of the final product, lead to excessive fat losses during churning, and cause curdling during heat treatment like pasteurization. The process involves adding alkaline substances to partially reduce this developed acidity, bringing the cream's pH closer to a neutral range, thereby enhancing its stability and sensory characteristics.

Purpose of Cream Neutralization

The primary objectives of cream neutralization are multifaceted and critical for producing high-quality dairy products, especially butter:

  • Reducing Fat Loss: High acidity in cream can lead to increased fat losses in buttermilk during churning, as casein entraps fat globules, causing them to be lost with the buttermilk. Neutralization helps minimize this.
  • Improving Flavor and Uniformity: Excessive acidity can result in undesirable off-flavors (e.g., sour or fishy notes) in butter. Neutralization helps to achieve a more consistent and desirable flavor profile.
  • Enhancing Keeping Quality: Butter made from high-acid cream deteriorates faster during storage. Neutralization to a suitable pH (typically 6.7 to 7.2 in butter serum) significantly improves its shelf stability.
  • Preventing Curdling: During pasteurization, high-acid cream is prone to curdling, which can damage processing equipment and affect product quality. Neutralization stabilizes the cream against heat coagulation.

Types of Neutralizing Agents

Alkaline compounds, commonly referred to as neutralizers, are used to reduce cream acidity. They are broadly classified into two types:

  • Lime Type Neutralizers: These include calcium oxides (quick limes), dolomitic or magnesium limes (magnesium and calcium oxides), and hydrated limes (slaked limes). Lime neutralizers are only partially soluble and are used as suspensions. They are generally stronger alkalis but can increase cream viscosity and may cause scorching if not used carefully. The neutralizing action of lime is also partially consumed by reacting with casein and phosphate, reducing its effective neutralizing capacity.
  • Soda Type Neutralizers: These are more frequently used and include sodium bicarbonate (baking soda), sodium carbonate (soda ash), caustic soda, and sodium sesquicarbonate. Soda neutralizers are generally preferred due to their better solubility and ease of handling. They react with acids to form salt, water, and carbon dioxide.

Process of Neutralization

The neutralization process involves several key steps to ensure effective acidity reduction without compromising cream quality:

  • Acidity Testing: The initial titratable acidity of the cream is determined (typically by titration with standard alkali using phenolphthalein indicator) to calculate the amount of neutralizer needed.
  • Calculation of Neutralizer: The quantity of neutralizer is precisely calculated based on the cream's initial acidity, desired final acidity, and the neutralizing factor of the chosen alkali.
  • Preparation and Addition: Neutralizers should never be added dry. They are diluted in clean potable water (10-15 times) to form a solution or suspension. This diluted neutralizer is then added slowly and evenly to the cream, ideally when the cream temperature is between 29°C to 32°C (85-90°F), with continuous vigorous stirring for 5-10 minutes to ensure uniform mixing and prevent localized over-neutralization.
  • Double Neutralization: For high-acid cream, a "double neutralization" method may be employed. This involves reducing the acidity in two stages, sometimes using a strong neutralizer (like lime or caustic soda) first to bring the acidity down to 0.3-0.4% lactic acid, followed by a milder soda neutralizer after pasteurization and cooling. This helps in managing carbon dioxide release and reducing intense flavor effects.
  • Post-Neutralization Pasteurization: After neutralization, the cream is usually pasteurized. Pasteurization further helps in completing the neutralization process by expelling carbon dioxide and destroying microorganisms.

Conclusion

Neutralization of cream is a fundamental practice in dairy technology, particularly for butter production, aimed at controlling acidity to ensure product quality, extend shelf life, and optimize processing efficiency. By carefully selecting and applying appropriate alkaline agents like lime or soda compounds, dairy processors can mitigate issues such as fat loss during churning and off-flavor development. This meticulous pH management ultimately contributes to consumer satisfaction and economic viability in the dairy industry, underscoring its importance in the manufacturing of various cream-based products.

Answer Length

This is a comprehensive model answer for learning purposes and may exceed the word limit. In the exam, always adhere to the prescribed word count.

Additional Resources

Key Definitions

Titratable Acidity
Titratable acidity refers to the total acidity of a dairy product, typically expressed as a percentage of lactic acid. It is determined by titrating a known volume of the sample with a standard alkaline solution (e.g., NaOH) in the presence of an indicator (e.g., phenolphthalein).
Neutralizing Factor
The neutralizing factor of an alkali is defined as the weight of the neutralizer required to react with one pound of lactic acid in the cream under plant conditions. This factor is crucial for accurately calculating the amount of neutralizer needed.

Key Statistics

For optimal keeping quality of salted butter, the acidity of cream is typically reduced to achieve a pH value of 6.7 to 7.2 in the butter serum.

Source: The Neutralization of Cream for Buttermaking - DSpace@GIPE

In practical applications, the neutralizing capacity of lime is approximately 80% of the theoretical amount, as about 20% reacts with casein and phosphate rather than lactic acid.

Source: Various-Process-_Cream.pptx - Slideshare

Examples

Common Neutralizers in Practice

Sodium bicarbonate (baking soda) and calcium hydroxide (slaked lime) are two of the most commonly used alkaline agents for neutralizing cream due to their effectiveness in raising pH by reacting with acids present in the cream.

Impact on Butter Flavor

Unneutralized, high-acid cream often leads to butter with a pronounced sour or "off" flavor. Proper neutralization helps in achieving a mild, clean, and desirable butter flavor, crucial for consumer acceptance.

Frequently Asked Questions

Why is complete neutralization to 0.0% acidity not desired?

Complete neutralization to 0.0% acidity would result in a very alkaline pH (around 8.3) in the butter, leading to an "alkaline" or "neutralized" flavor, which is undesirable. The goal is partial reduction to a near-neutral pH for optimal quality.

What is the effect of pasteurization on neutralized cream?

When cream neutralized with a soda compound is pasteurized, the titratable acidity might appear higher at churning due to retained carbon dioxide. However, this carbon dioxide has no significant effect on the pH of the butter serum, meaning the actual neutralization is effective.

Topics Covered

Food TechnologyDairy ScienceDairy ProductsMilk ProcessingFood Chemistry